SYNTHESIS AND CHARACTERIZATION OF NEW α-AMINOKETONE THIOSEMICARBAZONES

Authors

  • MSc. Félix A. Nápoles-Escutary Facultad de Ciencias Naurales, University of Oriente, Santiago de Cuba, Cuba
  • Lic. Rita M. Vale-Capdevilla Facultad de Ciencias Naurales, University of Oriente, Santiago de Cuba, Cuba
  • Dra. Magaly Casals-Hung Facultad de Ciencias Naurales, University of Oriente, Santiago de Cuba, Cuba
  • Lic. Jaciel La O-Rabionet Facultad de Ciencias Naurales, University of Oriente, Santiago de Cuba, Cuba
  • Jessica Joyce Facultad de Ciencias Naurales, University of Oriente, Santiago de Cuba, Cuba

Abstract

Novel thiosemicarbazones (4a-c) have been synthesized by condensation reaction of 2-(4-arylamino)-1,2-diphenyl-1-ethanones (3a-c) with thiosemicarbazide. Their structures were confirmed by elemental analysis, IR, 1HNMR, 13CNMR and MS spectra. The geometries were determined at the
Hartree-Fock level of theory employing 6-31G(d,p) basis set.
Keywords: thiosemicarbazone, α-aminoketone, synthesis, structure.

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Published

2015-11-10

How to Cite

Nápoles-Escutary, M. F. A., Vale-Capdevilla, L. R. M., Casals-Hung, D. M., La O-Rabionet, L. J., & Joyce, J. (2015). SYNTHESIS AND CHARACTERIZATION OF NEW α-AMINOKETONE THIOSEMICARBAZONES. Revista Cubana De Química, 24(3), 272–283. Retrieved from https://cubanaquimica.uo.edu.cu/index.php/cq/article/view/369

Issue

Vol. 24 No. 3 (2012)

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Artículos

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